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J. Korean Ceram. Soc. > Volume 43(9); 2006 > Article
Journal of the Korean Ceramic Society 2006;43(9): 588.
doi: https://doi.org/10.4191/kcers.2006.43.9.588
리튬이온전지용 LiMn2O4분말의 자전연소합성시 반응변수의 영향
장창현, Nersisyan Hayk, 원창환, 권혁상1
충남대학교 금속공학과
1한국과학기술원 신소재공학과
Effects of Reaction Parameters on the Preparation of LiMn2O4 for Lithium-Ion Batteries by SHS
Chang-Hyun Jang, Nersisyan Hayk , Chang-Whan Won, Hyuk-Sang Kwon1
Department of Metallurgical Engineering, Chungnam National University
1Department of Materials Science and Engineering, KAIST
Spinel phase $LiMn_2O_4$ is of great interest as cathode materials for lithium-ion batteries. In this study, SHS (Self propagating High-temperature Synthesis) method to synthesize spinel $LiMn_2O_4$ directly from lithium nitrate, manganese oxide, manganese and sodium chloride were investigated. The influence of Li/Mn ratio, the heat-treated condition of product have been explored. The resultant $LiMn_2O_4$ synthesized under the optimum synthesis conditions shows perfect spinel structure, uniform particle size and excellent electrochemical performances.
Key words: $LiMn_2O_4$, SHS method, Cycling test
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