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J. Korean Ceram. Soc. > Volume 40(10); 2003 > Article
Journal of the Korean Ceramic Society 2003;40(10): 998.
doi: https://doi.org/10.4191/kcers.2003.40.10.998
2.45 GHz 전자기파 조사하에서 Aluminum Borate Whisker의 성장 거동
김성완, 이상근, 김지경, 이창희, 안진모1, 신준식2, 박성수2, 박희찬
부산대학교 무기재료공학과
1삼성전기 복합부품팀
2부경대학교 화학공학부
Growth Behavior of Aluminum Borate Whisker under 2.45 GHz Electromagnetic Irradiation
ABSTRACT
With starting materials of two different powder mixtures, $Al_2$(S $O_4$)$_3$+xNa$_2$B$_4$ $O_{7}$$.$10$H_2O$(㏖ ratio; x=0.1, 0.7) and ${gamma}$-Al$_2$ $O_3$+xNa$_2$B$_4$ $O_{7}$$.$10$H_2O$(㏖ ratio; x=0.1, 0.7), whisker-type $Al_{18}$B$_4$ $O_{33}$ particles were synthesized by using conventional and microwave heat-treatment. The effects of microwave, amount of flux and temperature on the growth of whisker-type $Al_{18}$B$_4$ $O_{33}$ particles were investigated by using X-Ray Diffractometry (XRD) and Scanning Electron Microscopy (SEM). With increase of heat-treatment temperature and amount of flux, the size of whisker-type $Al_{18}$B$_4$ $O_{33}$ particles increased in both conventional and microwave heat-treated samples. However, compared to the conventional heat-treated samples, whisker-type $Al_{18}$B$_4$ $O_{33}$ particles were well grown for the microwave heat-treated samples.ted samples.
Key words: Microwave, $Al_{18}$$B_4$$O_{33}$ whisker, Flux, Synthesis
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