2.45 GHz 전자기파 조사하에서 Aluminum Borate Whisker의 성장 거동 |
김성완, 이상근, 김지경, 이창희, 안진모1, 신준식2, 박성수2, 박희찬 |
부산대학교 무기재료공학과 1삼성전기 복합부품팀 2부경대학교 화학공학부 |
Growth Behavior of Aluminum Borate Whisker under 2.45 GHz Electromagnetic Irradiation |
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ABSTRACT |
With starting materials of two different powder mixtures, $Al_2$(S $O_4$)$_3$+xNa$_2$B$_4$ $O_{7}$$.$10$H_2O$(㏖ ratio; x=0.1, 0.7) and ${gamma}$-Al$_2$ $O_3$+xNa$_2$B$_4$ $O_{7}$$.$10$H_2O$(㏖ ratio; x=0.1, 0.7), whisker-type $Al_{18}$B$_4$ $O_{33}$ particles were synthesized by using conventional and microwave heat-treatment. The effects of microwave, amount of flux and temperature on the growth of whisker-type $Al_{18}$B$_4$ $O_{33}$ particles were investigated by using X-Ray Diffractometry (XRD) and Scanning Electron Microscopy (SEM). With increase of heat-treatment temperature and amount of flux, the size of whisker-type $Al_{18}$B$_4$ $O_{33}$ particles increased in both conventional and microwave heat-treated samples. However, compared to the conventional heat-treated samples, whisker-type $Al_{18}$B$_4$ $O_{33}$ particles were well grown for the microwave heat-treated samples.ted samples. |
Key words:
Microwave, $Al_{18}$$B_4$$O_{33}$ whisker, Flux, Synthesis |
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