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J. Korean Ceram. Soc. > Volume 39(12); 2002 > Article
Journal of the Korean Ceramic Society 2002;39(12): 1149.
doi: https://doi.org/10.4191/kcers.2002.39.12.1149
압입법에 의한 실리콘의 상전이
김성순, 이홍림
연세대학교 세라믹공학과
Phase Transformation of Silicon by Indentation
Sung-Soon Kim, Hong-Lim Lee
Department of Ceramic Engineering, Yonsei University
ABSTRACT
Indentation was used to analyze high pressure phases of silicon. Phase transformations on both loading time and loading rate were studied. Micro-raman spectroscopy was used to observe the indentation-induced transformations. As the loading time increased, Si-III and Si-XII disappeared and only a-Si was observed in (111) samples. As the loading time increased, the residual stress was removed by creation of cracks or dislocations. At 0.1 mm/min loading rate, pop-in . At 5 mm/min loading rate pop-in was observed in force/displacement curve of (111) sample, but pop-in was not observed in force/displacement curve of (100) sample. This result indicates that the loading rate affects the volume of phase transformation in silicon.
Key words: Indentation, Holding time, Loading rate, Pop-in
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