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J. Korean Ceram. Soc. > Volume 35(8); 1998 > Article
Journal of the Korean Ceramic Society 1998;35(8): 857.
Glycine-Nitrate 법에 의한 BaTiO$_3$ 분말의 합성 및 그 특성(Part I)
박지애, 김구대1, 이홍림, 이동아1
연세대학교 세라믹공학과
1한국과학기술연구원 세라믹공정센터
Synthesis of the BaTiO$_3$ Powders by the Glyscine-Nitrate Process and Its Properties (Part I)
The BaTiO3 powders extensively used as MLCC (Multilayer ceramic capacitor) in electronic ceramic in-dustry were synthesized by GNP (Glycine-Nitrate process) The powders were prepared using carbonate and alkoxide as starting materials and nitric acid was used as a solvent for starting materials as well as an oxidant for combustion. The BaTiO3 powders were synthesized using different amounts of glycine as a fuel for combustion. The characteristics of synthesized powders were examined with helium pycnometer X-ray diffraction(XRD) Brunauer-Emmett-Teller with N2 adsorption and scanning electron microscopy(SEM). It was found that single phase BaTiO3 could be formed when the as-synthesized powders were heat-treated at 100$0^{circ}C$ When the glycine/cation molar ratio was 1,2 specific surface area was 24m2/g
Key words: Glycine-Nitrate process, BaTiO$_3$, Combustion
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