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J. Korean Ceram. Soc. > Volume 34(8); 1997 > Article
Journal of the Korean Ceramic Society 1997;34(8): 811.
화염 가수분해 증착에 의해 형성된 $SiO_2-P_2O_5-B_2O_3$ 유리 미립자의 특성
최춘기, 정명영, 최태구
한국전자통신연구원, 통신부품연구실
Characterization of $SiO_2-P_2O_5-B_2O_3$ Glass Soot fabricated by Flame Hydrolysis Deposition
SiO2-P2O5-B2O3 glass soot was fabricated by flame hydrolysis deposition and their properties by SEM, XRD, TGA-DSC were investigated., The mechanism of consolidation process of a glass soot as a function of consolidation temperature was analyzed by SEM observations. In the XRD patterns, the crystalline peaks which seem to be generated from B2O3 and BPO4 were observed. When the temperature of heat treatment exceeded 105$0^{circ}C$, the non-crystalline state of SiO2-P2O5-B2O3 glass was observed. In the TGA-DSC curves, the evaporation of water molecule by a sudden endothermic reaction was observed at 128$^{circ}C$ and a broad endothermic peak was seen in the temperature range of 40$0^{circ}C$-95$0^{circ}C$, without any weight loss. Finally, this peak was began to recover its baseline at 953$^{circ}C$. This point is equal to the temperature at which the densification begins. Furthermore, we observed that the addition of dopants such as P2O5 and B2O3 decrease the onset of consolidation temperature till 95$0^{circ}C$.
Key words: Flame hydrolysis deposition, Consolidation process, $SiO_2-P_2O_5-B_2O_3$ Glass Soot
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