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J. Korean Ceram. Soc. > Volume 30(12); 1993 > Article
Journal of the Korean Ceramic Society 1993;30(12): 987.
금속 Alkoxide를 이용한 LAS계 내열세라믹스의 제조에 관한 연구(I)
김형태, 이응상
한양대학교 무기재료공학과
Preparation of the LAS Ceramics for Heat Resistance using Metal Alkoxide (I)
ABSTRACT
In order to synthesize the heat resistance ceramics of LAS system, we studied on preparing the fine powder with homogeneity by sol-gel method using metal alkoxide. Various results were obtained depending on the composition and process. When the amount of H2O added at initial stage is higher than 10mol/$ell$, and when the amount of catalyst is 0.1mol/$ell$, the particle size of synthesized hydrate becomes finer. On condition that partial prehydrolysis time of TEOS is more than 50 hours, the monosized fine powder is obtained(below 1${mu}{textrm}{m}$).
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