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Journal of the Korean Ceramic Society 1991;28(6): 488. |
졸-겔법에 따른 실리카 유리 제조에 있어서 DCCA의 역할에 관한 연구 |
박용완, 연석주 |
한양대학교 공과대학 |
The Role of DCCA in the Sol-Gel Process Preparing Silica Glass |
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ABSTRACT |
In this study, the effects of catalyst and DCCA content were investigated in order to determine the optimum conditions of monolithic silica gel formation through sol-gel process. Formamide, oxalic acid, glycerol and dimethylformamide are used as DCCA. To observe the phenomena in drying and heat-treating of gels, we examined structural exchange of gels using FT-IR, TG-DTA and XRD. Monolithic gels were obtained by adding formamide and dimethylformamide as DCCA. According to the heat treatment schedule, silica glass is prepared by heat-treatment up to 1050$^{circ}C$. |
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