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J. Korean Ceram. Soc. > Volume 28(6); 1991 > Article
Journal of the Korean Ceramic Society 1991;28(6): 488.
졸-겔법에 따른 실리카 유리 제조에 있어서 DCCA의 역할에 관한 연구
박용완, 연석주
한양대학교 공과대학
The Role of DCCA in the Sol-Gel Process Preparing Silica Glass
ABSTRACT
In this study, the effects of catalyst and DCCA content were investigated in order to determine the optimum conditions of monolithic silica gel formation through sol-gel process. Formamide, oxalic acid, glycerol and dimethylformamide are used as DCCA. To observe the phenomena in drying and heat-treating of gels, we examined structural exchange of gels using FT-IR, TG-DTA and XRD. Monolithic gels were obtained by adding formamide and dimethylformamide as DCCA. According to the heat treatment schedule, silica glass is prepared by heat-treatment up to 1050$^{circ}C$.
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