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J. Korean Ceram. Soc. > Volume 23(4); 1986 > Article
Journal of the Korean Ceramic Society 1986;23(4): 78.
졸-겔법에 의한 지르코니아 섬유 제조 및 그 특성
이준, 김영정1, 황규홍2
서울대학교 무기재료공학과
1경상대학교 재료공학과
2서울대학교 재료공학과
Preparation of $ZrO_2$ Fibers by the Sol-Gel Process and its Properties
Zirconium acetate solution which was obtained from $ZrOCl_2$.$8H_2O$ was condensed polymerized and drawn to fibers by pulling method. Drawn gel fibers fired at 130$0^{circ}C$ were short porous and mechanically weak. But addition of CaO about 13m/o caused the fibers to have the cubic structure and relatively dense microstructure. In order to clarify the condition for the synthesis of zirconia fibers viscosity measurement DTA-TG analysis X-ray diffraction infrared spectroscopy, SEM and specific surface area were studied.
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