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Journal of the Korean Ceramic Society 1986;23(1): 67. |
제천규석으로부터 SiC 및 $SiC-Si_3N_4$계 분말 합성 |
이홍림, 배철훈, 문준화1 |
연세대학교 요업공학과 1아세아 시멘트(주) |
Syntheses of SiC and $SiC-Si_3N_4$ Powder from Jecheon Quartz |
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ABSTRACT |
SiC and $SiC-Si_3N_4$ powder were synthesized via the carbiding and carbiding-nitriding reaction of Jecheon quartz respectively using graphite as a reducing agent. $beta$-SiC+($alpha$+$beta$)-$Si_3N_4$ composite was obtained by the carbiding-nitriding reaction of Jecheon quartz-graphite mixture at 1, 35$0^{circ}C$ in $H_2$ atmosphere. $beta$-SiC+($alpha$+$beta$)-$Si_3N_4$ composite was obtained by the carbidint-nitriding reaction of Jecheon quartz-graphite mixture at 1, 35$0^{circ}C$ in $N_2-H_2$ atmosphere. The ratio of $beta$-SiC+($alpha$+$beta$)-$Si_3N_4$ content in a produced composite could be controlled by adjusting the reaction time and gaseous mixture. |
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