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Journal of the Korean Ceramic Society 1984;21(3): 278. |
| 초미립 $BaTiO_3$의 합성 |
| 안영필, 김복희, 황재석, 유경섭1 |
한양대학교 무기재료공학과
1경기공업개방대학 화학공학과 |
| Preparation of Submicron Barium Titanate Powders. |
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| ABSTRACT |
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Barium titanate powder was made by firing the complex hydroxide which had been synthesized with chemical wet process by the medium of $H_2O_2$. This experiment was done as following A mixed solution of $BaCl_2$, $TiCl_4$ and $H_2O_2$ with 1:1:10 mol ratio was prepared. Ammonium hydroxide was added into the mixed solution. In the range of pH 8-10 $BaTiO_3$ complex hydroxide was obtained and treated at room temperature 11$0^{circ}C$, 20$0^{circ}C$, 40$0^{circ}C$ and $600^{circ}C$. The results obtaiined from this experiment were as follows. At room temperature $BaTiO_3$ complex hydroxide was amorphous. Above 10$0^{circ}C$ crystalline $BaTiO_3$ was obtained and particle size of $BaTiO_3$ was increased with elevated temperature. So the particle size of BaTiO3 could be controlled by the firing temperature. After treating $BaTiO_3$ complex hydroxide at 10$0^{circ}C$ the average particle size of $BaTiO_3$ was 0.22$mutextrm{m}$ |
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